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81.
Qingzhao Yao Yuming Zhou Yanqing Sun Xiaoyun Ye 《Journal of Inorganic and Organometallic Polymers and Materials》2008,18(4):477-484
TiO2 hybrid molecular imprinted polymer (MIP) for ethofumesate using methacrylic acid (MAA) as the functional monomer and silane
coupling agent 3-(trimethoxysilyl) propylmethacrylate (KH570) as organic–inorganic connective bridge was synthesized via photo-excitation
method. Hydrogen bond was proved to act between MAA and ethofumesate for pre- and post-polymerization binding properties as
testified by UV spectrometric method. KH570 modified TiO2 nanoparticles were prepared via sonochemical reaction, which can accelerate hydrolysis, increase collision chance for the
reactive system and improve the dispersion of the nanoparticles. Scanning electron microscope (SEM), transmission electron
microscope (TEM), binding and the adsorption kinetics experiments as well as thermogravimetric analysis (TGA) were employed
for characterization. The results indicated that the hybrid MIP revealed a larger surface area and more ordered imprinting
cavities with improved thermal stability compared to organic-only MIP. Furthermore, faster adsorption kinetics and enhancive
adsorption capacity were achieved, which made it promising in chemical sensor applications. 相似文献
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83.
镁钴铝类水滑石催化合成安息香甲醚 总被引:1,自引:0,他引:1
采用共沉淀法制备了镁钴铝类水滑石化合物(MgCoAl-HTLcs),并用 X 射线衍射、扫描电子显微镜、NH_3程序升温脱附等方法对 MgCoAl-HTLcs 进行了表征,并以 MgCoAl-HTLcs 为催化剂催化苯甲醛与甲醇反应合成安息香甲醚,研究了n(Mg):n(Co):n(Al)、催化剂用量、原料配比、反应温度、反应时间对合成反应的影响。表征结果显示,MgCoAl-HTLcs 的晶相完整,表面主要为弱酸、弱碱性。催化合成安息香甲醚的适宜条件为:MgCoAl-HTLcs 催化剂用量0.10 g(约为原料总质量的0.23%),n(Mg):n(Co):n(Al)=0.4:1.6:1.0,V(苯甲醛):V(甲醇)=3:50,反应温度50℃,反应时间150 min。在此条件下,苯甲醛的平衡转化率达77.49%,安息香甲醚选择性接近100%。为洁净合成安息香甲醚开辟了一条新的途径。 相似文献
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Mixtures of Cr and Mo elemental powders, with the nominal compositions Cr25Mo75, Cr50Mo50, and Cr75Mo25, are processed by high-energy ball milling at ambient temperature. Milling is observed to force the mixing of the immiscible
bcc elements Cr and Mo into solid solutions. The lattice parameter of these solid solutions, measured by X-ray diffraction
(XRD), displays the expected positive deviation from Vegard’s law. These deviations are compared to the ones predicted by
Eshelby’s inclusion model for dilute alloys. The conventional Williamson-Hall approach is shown to fail to determine the grain
size in as-milled samples, probably due to the high density of dislocations. Annealing at 700 °C for 10 hours under argon
leads to a large reduction in structural defect density, without inducing any significant decomposition. The mixing measured
in Cr-Mo is discussed in the broader context of the mechanical mixing forced by ball milling in moderately immiscible systems. 相似文献
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89.
Fang Wu Yaojiang Zhang Zaw Zaw Oo Erping Li 《Antennas and Propagation Magazine, IEEE》2005,47(4):110-118
The Multilevel Fast Multipole Method (FMM) is a well-established method and can be applied to solve electromagnetic (EM) scattering problems. Compared with other traditional methods, it requires less computational time and memory. However, constrained by a single processor's speed and memory limitations, the problem size that can be solved by serial implementation is still relatively small. For a million-unknown target, the computational time on a single processor is intolerable, and memory could be easily exhausted. Parallel-computing technology, which can utilize multiprocessors, provides an efficient way to solve electrically large-scale EM problems. This paper will focus on discussing the parallel methodologies applied to a multilevel FMM code, as well as demonstrating the computational efficiency of the parallel approach. 相似文献
90.
该文介绍了Mall的产生条件和国内发展概况,并结合实例分析,着重论述建筑设计方面的有关问题。 相似文献